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Maxim Polikarpov Irina Snigireva John Morse Vyacheslav Yunkin Sergey Kuznetsov Anatoly Snigirev 《Journal of synchrotron radiation》2015,22(1):23-28
For the first time, single‐crystal diamond planar refractive lenses have been fabricated by laser micromachining in 300 µm‐thick diamond plates which were grown by chemical vapour deposition. Linear lenses with apertures up to 1 mm and parabola apex radii up to 500 µm were manufactured and tested at the ESRF ID06 beamline. The large acceptance of these lenses allows them to be used as beam‐conditioning elements. Owing to the unsurpassed thermal properties of single‐crystal diamond, these lenses should be suitable to withstand the extreme flux densities expected at the planned fourth‐generation X‐ray sources. 相似文献
33.
针对现代数字化战车电气与电子系统技术复杂、各分系统关联程度高、维修保障困难等问题,设计了一种基于CAN总线的数字化战车自动测试系统;整体设计基于模块化思想,充分利用车载备用总线,综合运用了DSP+FPGA控制处理技术、AFPN智能故障诊断技术,能够对车载电气与电子系统进行分系统独立测试和全系统联合检测,具有快速故障定位能力和拓扑适应能力;采用适配器与上位机测试软件的分体式设计,实现了平台物理资源复用。应用表明,该系统能够较好的适用于现代数字化战车的维修保障,使用方便,故障诊断快速有效。 相似文献
34.
本文介绍了在重水反应堆中进行应变测量的若干技术成果,主要是较好地解决了用在核辐射条件下,有水流冲刷的环境中的应用变计的粘贴与防护技术。在具有核辐射的环境中测试,通常选用聚酰亚胺胶作粘结剂。但是这种胶需在高温条件下固化,如果被测构件较大,是无法实现的。经测试筛选出具有防水防辐射性能的常温固化胶,并介绍了可用航空导线替代具有抗辐射性能的铠装电缆在堆内进行测量问题。采用有关措施后,经标定,在核辐射前后应 相似文献
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化学跑合剂对跑合效果的影响 总被引:1,自引:2,他引:1
在BJ52A胶合试验机、JP-BD1500型接触疲劳试验机和CL-100齿轮试验机上考察了化学跑合剂的作用,并就其机理进行了探讨。结果表明:采用化学跑合剂跑合后,表面粗糙度明显降低;表面接触面积增大,可以实现1次满载快速跑合;与采用含磨料的跑合方法比较,化学跑合剂可以明显提高表面接触精度,减少裂纹源的发生和发展,使表面承载能力明显提高。当齿轮加工精度较低或高速、重载齿轮的硬齿面精加工存在困难时,可 相似文献
37.
SiCp尺寸对SiCp/Cu基复合材料抗磨性能的影响 总被引:8,自引:1,他引:8
以纳米级(30nm)、亚微米级(130nm)、微米级(14μm)3种粒径的SiCp和微米级(10μm)铜粉为原料,用冷压烧结和热挤压方法制备了纳米、亚微米和微米级SiCp/Cu复合材料,考察了SiCp尺寸对SiCp/Cu复合材料抗磨性能的影响.结果表明,不同尺寸的SiCp颗粒作为增强相均能显著改善铜基复合材料的抗磨性能;随着SiCp尺寸的增大,SiCp/Cu复合材料的抗磨性能提高幅度显著增大,但偶件磨损表面的犁削加剧;以微米级SiCp为原料制备的SiCp/Cu复合材料的抗磨性能最佳,但其导致偶件40Cr钢犁削作用显著加剧.从摩擦副整体的摩擦磨损性能角度而言,宜采用SiCp尺寸为130nm的SiCp/Cu复合材料同40Cr钢组成摩擦副. 相似文献
38.
Interaction of PiB‐Derivative Metal Complexes with Beta‐Amyloid Peptides: Selective Recognition of the Aggregated Forms 下载免费PDF全文
Dr. André F. Martins David M. Dias Dr. Jean‐François Morfin Dr. Sara Lacerda Dr. Douglas V. Laurents Dr. Éva Tóth Prof. Carlos F. G. C. Geraldes 《Chemistry (Weinheim an der Bergstrasse, Germany)》2015,21(14):5413-5422
Metal complexes are increasingly explored as imaging probes in amyloid peptide related pathologies. We report the first detailed study on the mechanism of interaction between a metal complex and both the monomer and the aggregated form of Aβ1–40 peptide. We have studied lanthanide(III) chelates of two PiB‐derivative ligands (PiB=Pittsburgh compound B), L1 and L2, differing in the length of the spacer between the metal‐complexing DO3A macrocycle (DO3A= 1,4,7,10‐tetraazacyclododecane‐1,4,7‐triacetic acid) and the peptide‐recognition PiB moiety. Surface plasmon resonance (SPR) and saturation transfer difference (STD) NMR spectroscopy revealed that they both bind to aggregated Aβ1–40 (KD=67–160 μM ), primarily through the benzothiazole unit. HSQC NMR spectroscopy on the 15N‐labeled, monomer Aβ1–40 peptide indicates nonsignificant interaction with monomeric Aβ. Time‐dependent circular dichroism (CD), dynamic light scattering (DLS), and TEM investigations of the secondary structure and of the aggregation of Aβ1–40 in the presence of increasing amounts of the metal complexes provide coherent data showing that, despite their structural similarity, the two complexes affect Aβ fibril formation distinctly. Whereas GdL1, at higher concentrations, stabilizes β‐sheets, GdL2 prevents aggregation by promoting α‐helical structures. These results give insight into the behavior of amyloid‐targeted metal complexes in general and contribute to a more rational design of metal‐based diagnostic and therapeutic agents for amyloid‐ associated pathologies. 相似文献
39.
Xinpeng Li Chao Guo Yu Zhang Kejun Liu 《Journal of Macromolecular Science: Physics》2015,54(2):215-229
The pressure vibration injection molding (PVIM) method was used to prepare β-nucleated isotactic polypropylene samples (PVIM β-iPP samples); a relatively low, periodical shear was imposed on the polymer melt in the mold at the filling and packing stages. The crystal structures and crystal orientation of the PVIM β-iPP samples were investigated by polarizing light microscopy (PLM), scanning electron microscopy (SEM), and synchrotron two-dimensional wide-angle X-ray diffraction (2D-WAXD). The PLM observations indicated that a cylindrite layer, rather than the transition layer, was found in PVIM β-iPP samples, which is different from the conventional injection-molded (CIM) samples. In addition, the thickness of the oriented layer of the PVIM samples was obviously greater than that of the CIM samples. The SEM observations demonstrated that a large amount of shish-kebab structures appeared in the shear layer of the PVIM β-iPP samples; at the same time, numerous β-spherulites were formed in the core layer. The 2D-WAXD data indicated that orientation homogeneity, to some degree, could be obtained by the periodical shear during PVIM. As a result, the above-mentioned morphology of the PVIM β-iPP samples leads to potentially useful prominent reinforcement and toughening of the material. 相似文献
40.
Dr. Yi Luo Dr. Stef Smeets Dr. Zhendong Wang Prof. Junliang Sun Prof. Weimin Yang 《Chemistry (Weinheim an der Bergstrasse, Germany)》2019,25(9):2184-2188
A new germanosilicate zeolite named SCM-15 (Sinopec Composite Material No. 15), the first zeolite containing a 3-dimensional (3D) channel system with interconnected 12-, 12-, and 10-ring channels (pore sizes: 6.1×7.2, 6.1×7.4, and 5.2×5.9 Å), has been synthesized using neutral 4-pyrrolidinopyridine as organic structure-directing agents (OSDAs). Its structure has been determined by combining single-crystal electron diffraction (SCED) and synchrotron powder X-ray diffraction (SPXD) data. The unique open framework structure of SCM-15 is related to that of FOS-5 ( BEC ), ITQ-7 ( ISV ), PKU-16 ( POS ), ITQ-26 ( IWS ), ITQ-21, Beta polymorph B, and SU-78B, since all these framework structures can be constructed from similar chains which are connected through shared 4-ring or double 4-ring (d4r) units. Based on this relation, six topologically reasonable 3D large or extra-large pore hypothetical zeolites are predicted. 相似文献